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For instance, it is usually impossible to fully invert quadrupole spins I > 1/2 by a 180◦ -pulse. The rotational echo adiabatic passage double resonance (REAPDOR) experiment circumvents this problem by applying a prolonged pulse to the I spins that inverts these spins with higher efficiency than a 180◦ pulse [59]. The prolonged pulse achieves inversion since during rotation the resonance frequency of the I spins adiabatically passes the frequency of the applied pulse. The PISEMA experiment introduced in the previous section can also be applied under MAS conditions [60].

A) A. J. de Haas: Verhandl. Deut. Phsik. Ges. 17, 152–170 (1915) (b) A. J. de Haas: Verhandl. Deut. Phsik. Ges. 18, 173–177 (1916) 6. H. Van Vleck: The Theory of Electric and Magnetic Susceptibility (Clarendon, Oxford 1932) pp 94–97 7. B. I. F. R. Zacharias: Phys. Rev. 56, 728–743 (1939) 8. (a) F. W. Hansen, M. Packard: Phys. Rev. M. C. V. Pound: Phys. Rev. 69, 37–38 (1946) 9. A. Abragam, B. Bleaney: Electron Paramagnetic Resonance of Transition Ions (Clarendon, Oxford 1970) 10. M. Purcell: Astrophys.

K. H. Waugh: Phys. Rev. B 52, 6467–6469 (1995) 13. B. Black, B. Majer, A. Pines: Chem. Phys. Lett. 201, 550–554 (1993) 14. L. L. Hahn: Phys. Rev. 133, A1616–A1629 (1964) 15. A. Abragam: Principles of Nuclear Magnetism (Clarendon, Oxford 1961) 16. M. Goldman: Spin Temperature and Nuclear Magnetic Resonance in Solids (Clarendon, Oxford 1970) Distance Measurements in Solid-State NMR and EPR Spectroscopy G. W. de Abstract. Magnetic resonance techniques for the measurement of dipole-dipole couplings between spins are discussed with special emphasis on the underlying concepts and on their relation to site-specific distance determination in complex materials.

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